Journal
MATERIALS
Volume 13, Issue 8, Pages -Publisher
MDPI
DOI: 10.3390/ma13081810
Keywords
titanium; ball milling; powder; self-propagating high-temperature synthesis; carbonitride
Categories
Funding
- Integration Program of Fundamental Research of the Siberian Branch of the Russian Academy of Sciences [KP 25.5]
- Ministry of Science and Higher Education of the Russian Federation [AAAA-A17-117030310277-6]
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In this work, titanium carbonitrides were synthesized by self-propagating high-temperature synthesis (SHS) in nitrogen. For the first time, the synthesis of titanium carbonitrides by combustion was realized in nitrogen at atmospheric pressure. The synthesis was carried out by subjecting high-energy ball-milled titanium-carbon black powder mixtures to combustion in a nitrogen atmosphere. The influence of the ball milling time on the phase composition of the products of SHS conducted in the Ti+0.3C reaction mixture was studied. It was found that the titanium-carbon black mixtures need to be milled for a certain period of time for the combustion synthesis to yield a single-phase carbonitride product.
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