Journal
NATURE COMMUNICATIONS
Volume 11, Issue 1, Pages -Publisher
NATURE PUBLISHING GROUP
DOI: 10.1038/s41467-020-16351-0
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Funding
- National Science Foundation through the University of Pittsburgh [NSF DMR 1808046]
- NSF [CMMI 1635088]
- U.S. Department of Energy, Office of Biological and Environmental Research
- U.S. Department of Energy [DE-AC05-76RLO1830]
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Design and processing of advanced lightweight structural alloys based on magnesium and titanium rely critically on a control over twinning that remains elusive to date and is dependent on an explicit understanding on the twinning nucleation mechanism in hexagonal close-packed (HCP) crystals. Here, by using in-situ high resolution transmission electron microscopy, we directly show a dual-step twinning nucleation mechanism in HCP rhenium nanocrystals. We find that nucleation of the predominant {1 0 -1 2} twinning is initiated by disconnections on the Prismatic Basal interfaces which establish the lattice correspondence of the twin with a minor deviation from the ideal orientation. Subsequently, the minor deviation is corrected by the formation of coherent twin boundaries through rearrangement of the disconnections on the Prismatic|Basal interface; thereafter, the coherent twin boundaries propagate by twinning dislocations. The findings provide high-resolution direct evidence of the twinning nucleation mechanism in HCP crystals. Aspects of twinning in hexagonal-close-packed crystals remain elusive. Here, the authors directly image twinning in rhenium nanocrystals and show the process is mediated by disconnections on Prismatic|Basal interfaces as the twin initially deviates from its ideal orientation before it is corrected.
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