Journal
ORGANIC LETTERS
Volume 22, Issue 8, Pages 3185-3189Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c00944
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Funding
- JSPS KAKENHI [JP 18K19078, JP 17H06092]
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We have developed a new strategy for the generation of phosphenium dication equivalents from readily available phosphinic acids and Tf2O. The in situ-generated dication equivalents can be readily coupled with simple (hetero)biaryls to form the corresponding dibenzophospholes directly. This protocol can also be applied to the concise synthesis of six- and seven-membered phosphacycles as well as the largely pi-extended heteroacene derivatives, which are of great interest in the field of organic functional materials.
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