Journal
ORGANIC LETTERS
Volume 22, Issue 8, Pages 3110-3113Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c00858
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Funding
- National Natural Science Foundation of China [21971263]
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A C-2-symmetric chiral spirocyclic diol aza-SPINOL containing a spirooxindole scaffold has been designed, synthesized, and optically resolved. The product could be synthesized on gram scale in an overall yield of 22%. Moreover, elaborations of aza-SPINOL to other chiral ligands as well as the preliminary investigation of the related bisphosphine ligand in the desymmet-rization of bisallylic amide were reported.
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