Journal
ORGANIC LETTERS
Volume 22, Issue 6, Pages 2333-2338Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c00532
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Funding
- NNSFC [21971081, 91856119, 21622201, 21820102003, 91956201, 21772053]
- Science and Technology Department of Hubei Province [2017AHB047]
- Program of Introducing Talents of Discipline to Universities of China (111 Program) [B17019]
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A visible-light-driven, copper-catalyzed C(sp(3))-O coupling of benzylic radicals with phenols is described for the first time. This operationally simple and robust process features mild conditions, broad scope, and high functional-group tolerance, enabling the construction of a diverse range of cyanoalkylated aryl ethers (33 examples). Key to this protocol is the dual role of copper salt that acts not only as a photosensitizer but also as a cross-coupling catalyst.
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