4.7 Review

Standardization of the minimum information for publication of infrared-related data when microplastics are characterized

Journal

MARINE POLLUTION BULLETIN
Volume 154, Issue -, Pages -

Publisher

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.marpolbul.2020.111035

Keywords

Microplastics; Infrared spectrometry; Standardization; Information; Reproducibility crisis; Quality control

Funding

  1. Spanish Ministry of Economy and Competitiveness, JPI-Oceans BASEMAN project - European Regional Development Fund program [PCIN-2015-170-C02-01, CTM2016-77945-C3-3-R]
  2. Program 'Consolidacion e Estructuracion de Unidades de Investigacion Competitiva' of the Galician Government (Xunta de Galicia) [ED431C 2017/28]

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Infrared spectrometry (IR) became a workhorse to characterize microplastics (MPs) worldwide. However, reports on the experimental conditions to measure them decreased alarmingly. As complete, relevant information on the instrumental setup determining IR spectra is crucial for scientific reproducibility, ca. 50% of the papers that reported FTIR to measure MPs were evaluated and it was found that most studies cannot be replicated due to missing experimental details. To ameliorate this, the most critical parameters influencing IR spectra are depicted, their impact when matching a spectrum against databases exemplified, and, following efforts from other scientific fields, a minimum information for publication of IR-related data on MPs characterization (MIPIR-MP) is proposed, along with a brief, simple paragraph to resume the most critical information to be reported. This can be used to improve the worrying figures that point out to a reproducibility crisis in the field, as disclosed by the survey.

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