Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 85, Issue 9, Pages 5959-5972Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.0c00326
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Funding
- JSPS KAKENHI [JP16K18844, JP17J00025]
- Futaba Electronics Memorial Foundation
- Suzuken Memorial Foundation
- Inamori Foundation
- Daiichi Sankyo Foundation of Life Science
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Furoxans are potentially useful heteroaromatic units in pharmaceuticals and agrichemicals. However, the applications for furoxan-based compounds have been hampered due to the underdevelopment of their synthetic methods. Herein, we report a new synthetic approach for the synthesis of chloro- and bromofuroxans. The starting materials were dichloro- and dibromofuroxans, and the substituents were directly introduced to the furoxan ring in a modular fashion. The synthesized monohalofuroxans served as substrates for the installation of a second substituent to prepare further functionalized furoxans.
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