Journal
CHEMICAL COMMUNICATIONS
Volume 52, Issue 76, Pages 11446-11449Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cc06200h
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Funding
- NSFC [21602182]
- Sichuan Provincial Science and Technology Department [2016TD0014]
- Sichuan Provincial Education Department [16ZB0133]
- Open Project of MSKL [11zxfk26, 13zxfk06, 14tdfk03]
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A palladium catalyzed/silver tuned selective mono- and tetra-acetoxylation of o-carboranes has been developed, and a series of mono- and tetra-acetoxylated o-carboranes decorated with active groups have been synthesized with moderate to good yields as well as excellent selectivity. A mechanism involving electrophilic palladation and cyclopalladation of the B-H bond was proposed.
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