Journal
JOURNAL OF ELECTRONIC MATERIALS
Volume 49, Issue 8, Pages 4754-4763Publisher
SPRINGER
DOI: 10.1007/s11664-020-08191-x
Keywords
Nonenzymatic; glucose sensor; Au nanoparticles; metal organic frameworks
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Funding
- National Natural Science Foundation of Zhejiang Province [LY12B07001]
- Xinmiao Talent Project of Zhejiang Province [2018R407073]
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Au nanoparticles were decorated on Ni-based metal-organic frameworks to improve their electrochemical performance for nonenzymatic glucose detection through a convenient and fast microwave-assisted process. Various techniques including scanning electron microscopy, transmission electron microscopy, X-ray diffraction, energy dispersive X-ray mapping and X-ray photoelectron spectroscopy were used to characterize the Au@Ni-BTC composites. The results revealed that Au nanoparticles were uniformly deposited on the Ni-BTC microspheres. The constructed Au@Ni-BTC sensors showed highly increased glucose detection performance with a wide linear range (5-7400 mu M), high sensitivity (1447.1 mu A mM(-1) cm(-2)) and low detection limit (1.5 mu M). Moreover, they also exhibited good selectivity and preferable feasibility for serum sample analysis. The improved glucose sensing performance may be due to the synergistic effects of Au nanoparticles and Ni-BTC, which facilitated faster charge transfer in the electrochemical process. The study of Au@Ni-BTC may also provide a promising material for constructing highly efficient nonenzymatic glucose sensors.
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