Journal
CHEMICAL COMMUNICATIONS
Volume 52, Issue 25, Pages 4632-4635Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cc01074a
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- EPSRC
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Using the DP4f GIAO-NMR method, the stereochemistry of hemicalide was computationally analysed, resulting in a reassignment at C18 as supported by improved NMR shift correlations with a model C13-C25 fragment 23. An advanced C16-C28 subunit 6 of this potent anticancer agent was then synthesised with the revised 18,19-syn relationship.
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