Journal
INORGANIC MATERIALS
Volume 56, Issue 2, Pages 126-131Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0020168520020065
Keywords
nanoparticle; vanadium diboride; autoclave reactor; sodium borohydride; vanadium(III) chloride
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Funding
- Russian Federation Ministry of Science and Higher Education [0089-2019-0007]
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It has been shown using X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, energy dispersive X-ray spectroscopy, and elemental analysis that phase-pure VB2 with an average particle size in the range 20-35 nm can be prepared in the temperature range 595-930 degrees C by reacting vanadium(III) chloride and sodium borohydride in the molar ratio 1 : 10 in an argon atmosphere for 14-28 h.
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