Journal
ORGANOMETALLICS
Volume 39, Issue 5, Pages 636-639Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.organomet.0c00013
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- Universite de Montpellier
- Centre Nationale de la Recherche Scientifique (CNRS)
- Agence Nationale de la Recherche [ANR-16-CE07-0009-01]
- Agence Nationale de la Recherche (ANR) [ANR-16-CE07-0009] Funding Source: Agence Nationale de la Recherche (ANR)
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The use of ball mills enabled the efficient mechanosynthesis of a variety of N-aryl,N-alkyl imidazolium salts and of corresponding NHC silver(I) complexes. Transmetalation with ruthenium via mechanochemistry allowed the rapid access (from 1.5 min to 1 h) to complexes having a similar structure to Noels-type precatalysts. Evaluation of the complexes in the ring-opening metathesis polymerization of norbornene in different solvent, including nontoxic ones, showed a high catalytic activity for one of them, comparable to that of the Noels catalyst.
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