Journal
ORGANIC LETTERS
Volume 22, Issue 3, Pages 896-901Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b04448
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Funding
- University of Kansas Office of the Provost
- Department of Medicinal Chemistry
- COBRE Protein Structure and Function Small Grants Program
- NIH Shared Instrumentation Grant [S10RR014767]
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This communication discloses the first examples of aza-Wacker cyclizations of sulfamate esters. Within the realm of related cyclization reactions, this protocol is differential in that it forms six-membered rings in good yield and uses catalytic amounts of palladium(0) rather than palladium(II) salts. These reactions scale well, and their products are demonstrated to be valuable synthetic intermediates.
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