Journal
ORGANIC LETTERS
Volume 22, Issue 3, Pages 902-907Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b04450
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Funding
- Freie Universitat Berlin (Forschungskommissionsmittel)
- DFG
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A scalable access to functionalized ferrocenyl azides has been realized in flow. By halogen-lithium exchange of ferrocenyl halides and trapping with tosyl azide, a variety of functionalized ferrocenyl azides were obtained in high yields. To allow a scalable preparation of these potentially explosive compounds, a flow protocol was developed accelerating the reaction time to minutes and circumventing accumulation of potentially hazardous intermediates. The corresponding ferrocenyl amines were then prepared by a reliable reduction process.
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