Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 85, Issue 2, Pages 1224-1231Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b02535
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Funding
- National Science Foundation of China [21572158]
- Tianjin Natural Science Foundation [18JCQNJC76600]
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A novel visible-light photocatalytic difluoromethylselenolation of aryl amines via in situ generation of aryldiazonium salts was achieved using Se-(difluoromethyl) 4-methylbenzene-sulfonoselenoate, which was synthesized for the first time. The reagent is readily accessible and shelf-stable. The metal-free reaction conditions and the broad substrate scope provide a green protocol for the efficient and rapid introduction of the difluoromethylselenylether group.
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