4.5 Article

Development of SrFe12O19/Ti3SiC2 Composites for Enhanced Microwave Absorption

Journal

JOURNAL OF ELECTRONIC MATERIALS
Volume 49, Issue 3, Pages 2233-2241

Publisher

SPRINGER
DOI: 10.1007/s11664-019-07922-z

Keywords

Composite materials; sol-gel processes; magnetization; magnetic measurements

Funding

  1. Directorate of Extramural Research & Intellectual Property Rights, DRDO, New Delhi
  2. UGC, New Delhi

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Microwave absorbing composites containing strontium hexaferrite and titanium silicon carbide, SrFe12O19/Ti3SiC2 powder, were synthesized by mixing in different weight ratios. The strontium hexaferrite (SrFe12O19) particles were synthesized using low-temperature combustion. The 'as synthesized' strontium hexaferrite powder is observed to have low coercivity (255.09 G) and high saturation magnetization (45.1 emu/g). The titanium silicon carbide (Ti3SiC2) powder was synthesized by heat treatment of the precursors (Ti/Si/TiC) at 1100 degrees C under argon atmosphere. A microwave absorbing composite is fabricated by mixing in a high-energy ball mill followed by heating of SrFe12O19 and Ti3SiC2 powders at 200 degrees C. The maximum reflection loss of -39.67 dB is observed at 9.46 GHz for the composite casted into pellets containing 20% Ti3SiC2 and 80% SrFe12O19 with 2-mm thickness. The bandwidth for less than -10 dB loss is observed to be 2.77 GHz (66% of the total band). The developed magneto-dielectric composition confirmed its candidacy as a potential microwave absorbing material.

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