4.1 Article

Developments of nano-polycrystalline diamond anvil cells for neutron diffraction experiments

Journal

HIGH PRESSURE RESEARCH
Volume 40, Issue 1, Pages 184-193

Publisher

TAYLOR & FRANCIS LTD
DOI: 10.1080/08957959.2020.1727465

Keywords

Neutron diffraction; nano-polycrystalline diamond; high pressure

Funding

  1. Japan Society for the Promotion of Science (JSPS KAKENHI) [18H05224, 18H01936, 15H05829]
  2. JSPS-CNRS bilateral joint research project [PRC2191]
  3. Grants-in-Aid for Scientific Research [18H01936] Funding Source: KAKEN

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A new high pressure cell for neutron diffraction experiments using nano-polycrystalline anvils is presented. The cell design, off-line pressure generation tests and a gas-loading procedure for this cell are described. The performance is illustrated by powder neutron diffraction patterns of ice VII to similar to 82 GPa. We also demonstrate the feasibility of single crystal neutron diffraction experiments of Fe3O4 at ambient conditions using this cell and discuss the current limitation and future developments.

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