Journal
ACS APPLIED MATERIALS & INTERFACES
Volume 12, Issue 6, Pages 7381-7391Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acsami.9b13362
Keywords
phosphorene; black phosphorus; high-pressure synthesis; exfoliation; transport properties; ceramic; nanostructures
Funding
- Czech Science Foundation (GACR) [18-12761S, 19-26910X]
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Black phosphorus is currently among the most explored two-dimensional (2D) materials. Currently, the synthesis methods are dominantly based on vapor-phase growth of black phosphorus. In this manuscript, we demonstrate large-scale synthesis of black phosphorus by rapid high-pressure transition of red phosphorus. The high-pressure conversion of red phosphorus led to high-density nanocrystalline black phosphorus ceramics. The resulting material was explored in detail including structural and morphological characterization in addition to thermal and electrical transport and basic thermophysical properties. The nanocrystalline black phosphorus can be employed for large-scale production of stable few/single-layer black phosphorus colloidal solutions in various solvents.
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