4.7 Article

Effect of addition of small amounts of samarium on microstructural evolution and mechanical properties enhancement of an as-extruded ZK60 magnesium alloy sheet

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ELSEVIER
DOI: 10.1016/j.jmrt.2019.10.038

Keywords

As-extruded Mg-5.5Zn-0.8Zr alloy; Samarium; Microstructure; Mechanical properties

Funding

  1. National Natural Science Foundation of China [51804189]
  2. Shandong University of Technology [4041-414014]
  3. Project of Science and Technology Development Plan of Zibo City, Shandong Province [9001-111088]
  4. Research Award Fund for Outstanding Young and Middle-aged Scientists of Shandong Province [ZR2016EMB22]
  5. Shandong Natural Science Foundation [ZR2015PE002, ZR2017BEM004, ZR2017MEE038]

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The microstructure, texture evolution and mechanical properties of as-extruded Mg-5.5Zn-0.8Zr (wt.%) (ZK60) alloy with 1 % Sm addition were investigated. The results showed that the as-extruded ZK60-1Sm alloy consisted of alpha-Mg, Mg2Zn3, Mg7Zn3, Mg41Sm5 and (Mg, Zn)(3)Sm phases. The addition of 1 %Sm precipitated the Mg(41)Sm(5)and (Mg, Zn)(3)Sm phases, which promoted the dynamic recrystallization (DRX) in the subsequent extrusion process and resulted in grain refinement. The microtexture and the orientation distribution characteristic implied that large amounts of < 01-10 > and <-12-10 > slips were activated in ZK60-1Sm alloy during extrusion process, while only < 01-10 > basal slip was observed in ZK60 alloy. The non-basal slips led to more potential nucleation sites and a better coordination for the deformation, resulting in the better comprehensive mechanical properties of the as-extruded ZK60-1Sm sheet. Meanwhile, the as-extruded ZK60-1Sm alloy showed higher strength and ductility compared to ZK60 alloy. The ultimate tensile strength (UTS), the yield strength (YS) and the elongation to failure (EL) along the extrusion direction (ED) were enhanced by 11.7 %, 24.5 % and 26.2 %, respectively. The influence of fine grain microstructure, nanoscale Mg 4 iSms phase, micron scale (Mg, Zn) 3 Sm phase and texture evolution, contributed mainly to the strength of as-extruded ZK60-1Sm alloy. (C) 2019 The Authors. Published by Elsevier B.V.

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