Journal
ACS MACRO LETTERS
Volume 8, Issue 11, Pages 1437-1441Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acsmacrolett.9b00767
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Funding
- Fonds Wetenschappelijk Onderzoek (FWO)
- Faculty of Science (Monash University)
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An automated polymer synthesis platform based on an inline low-field nuclear magnetic resonance spectrometer is developed. Flow chemistry and automated inline analyses are an excellent combination for automated kinetic screening and for self-optimizing reactions with programmable conversion targeting. By monitoring monomer conversion over a continuous range of reactor residence times, the platform is able to construct kinetic profiles of polymerizations in an accurate and efficient way. The machine assisted self-optimization routine allows the reaction to be stopped at any given preselected conversion, giving rise to unprecedented reproducibility in polymer synthesis.
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