Journal
TETRAHEDRON LETTERS
Volume 60, Issue 43, Pages -Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2019.151124
Keywords
Visible-light photoredox catalysis; Eosin Y; Perfluoroalkylation; Hydrazones
Categories
Funding
- National Natural Science Foundation of China [21702087, 21801105]
- Natural Science Foundation of Liaoning Province [2015020196, 20170520353, 20180510033]
- Program for Liaoning Innovative Talents in University [LR2017021]
- Research Project Fund of Liaoning Provincial Department of Education [L2017LQN010, L2017LZD001]
- Talent Scientific Research Fund of Liaoning Shihua University [2016XJJ-078, 2016XJJ-079]
- open project of Jilin Province Key Laboratory of Organic Functional Molecular Design Synthesis [130028836, 130028911]
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A general and facile visible-light-promoted organic dye catalyzed perfluoroalkylation of hydrazones has been developed using inexpensive and non-toxic Eosin Y as the photoredox catalyst under mild conditions. This reaction protocol exhibits synthetic simplicity, broad scope of substrates, and excellent functional group compatibility. A gram scale synthesis can be also facilitated with a satisfactory yield, which opens up the possibility of practical applications. (C) 2019 Elsevier Ltd. All rights reserved.
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