Journal
SYNTHESIS-STUTTGART
Volume 52, Issue 5, Pages 711-718Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0039-1691486
Keywords
electrochemical reaction; thiocyanation; enaminones; oxidant- free; catalyst free
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Funding
- Natural Science Foundation of Hunan Province [2019JJ50214]
- Joint Funds of Hunan Province Engineering Research Center of Radioactive Control Technology in Uranium Mining and Metallurgy & Hunan Province Engineering Technology Research Center of Uranium Tailings Treatment Technology [2019YKZX2012]
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A simple and efficient electrochemically induced thiocyanation of enaminones under undivided electrolytic conditions has been developed. With this protocol, various polyfunctionalized alkenes and chromones could be obtained in good to excellent yields using readily available KSCN as the thiocyanation reagent under catalyst-, oxidant-, and transition-metal-free conditions.
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