Journal
ORGANIC LETTERS
Volume 21, Issue 20, Pages 8449-8453Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b03216
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Funding
- NIH [5R01AG039468]
- CRIF program of the National Science Foundation [CH E9974921]
- Elsa Pardee Foundation
- University of Hawaii at Manoa
- Department of Defense [W911NF-04-1-0344]
- MRI grant from the National Science Foundation [1532310]
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1532310] Funding Source: National Science Foundation
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The bioactivity-guided examination of a Leptolyngbya sp. led to the isolation of leptazolines A D (1-4), from the culture media, along with two degradation products (5 and 6). Density functional theory nuclear magnetic resonance calculations established the relative configurations of 1 and 2 and revealed that the calculated shifts depended on the operating system when using the Willoughby Hoye Python scripts to streamline the processing of the output files, a previously unrecognized flaw that could lead to incorrect conclusions.
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