Journal
BIOMACROMOLECULES
Volume 17, Issue 6, Pages 1921-1929Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.biomac.6b00257
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Funding
- PRESTO program from Japan Science and Technology Agency (JST)
- Project for Creation of Research Platforms and Sharing of Advanced Research Infrastructure by the Ministry of Education, Culture, Sports, Science, and Technology of Japan (MEXT)
- Grants-in-Aid for Scientific Research [15K14767] Funding Source: KAKEN
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A 4-O-5-tetramer lignin model compound carrying beta-O-4 linkages on each Of the side-chain Moieties was synthesized, as well as 4-O-5-coupled dehydrodiconiferyl alcohol. By comparison with theiriNMR,data, two cross signals in the HSQC spectrum Of pane milled wood lignin recorded in DMSO-d(6) were assigned-to H2/C2 and H6/C6 correlations on the aromatic rings of 4-O-5-linke.d units; Although the H2/C2 correlation peak- appeared in the same region as syringyl units, nitrobenzene-oxidation of the pine lignin did not yield any syringyl-type product, but did release a 4-O-5-type product.
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