4.4 Article

Coinage metal catalyzed 7-endo-trig cyclization of ene-diols: Construction of 2,2-dimethyloxepane frameworks

Journal

TETRAHEDRON LETTERS
Volume 60, Issue 36, Pages -

Publisher

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2019.151038

Keywords

Silver; Ene-diol; Cyclization; Gold

Funding

  1. JSPS KAKENHI [JP18H04244, JP17k08209]

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The silver catalyzed 7-endo-trig cyclization of an ene-diol for the formation of 2,2-dimethyloxepane frameworks has been developed. The spirotype dioxabicyclic products were also produced from the diene-diols. In addition, a gold catalyst featuring the Z-ligand also produced similar cyclization reactions. (C) 2019 Published by Elsevier Ltd.

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