Journal
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
Volume 12, Issue -, Pages 1096-1100Publisher
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.12.104
Keywords
bifunctional organocatalyst; enantioselective Michael addition; keramaphidin B; nitro-Mannich lactamisation cascade
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Funding
- EPSRC [EP/M50659X/1]
- EPSRC [EP/G007802/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [1112321, EP/G007802/1] Funding Source: researchfish
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The enantio-and diastereoselective Michael addition of a delta-valerolactone-derived pronucleophile to a substituted furanyl nitroolefin catalysed by a bifunctional cinchonine-derived thiourea has been used as the key stereocontrolling step in a new synthetic strategy to the heavily functionalised piperidine core of keramaphidin B.
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