4.5 Article

The Velociprobe: An ultrafast hard X-ray nanoprobe for high-resolution ptychographic imaging

Journal

REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 90, Issue 8, Pages -

Publisher

AMER INST PHYSICS
DOI: 10.1063/1.5103173

Keywords

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Funding

  1. Argonne LDRD [2015-153-N0]
  2. DOE Office of Science [DE-AC02-06CH11357]
  3. Office of the Director of National Intelligence (ODNI), Intelligence Advanced Research Projects Activity (IARPA)

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Motivated by the advanced photon source upgrade, a new hard X-ray microscope called Velociprobe has been recently designed and built for fast ptychographic imaging with high spatial resolution. We are addressing the challenges of high-resolution and fast scanning with novel hardware designs, advanced motion controls, and new data acquisition strategies, including the use of high-bandwidth interferometric measurements. The use of granite, air-bearing-supported stages provides the necessary long travel ranges for coarse motion to accommodate real samples and variable energy operation while remaining highly stable during fine scanning. Scanning the low-mass zone plate enables high-speed and high-precision motion of the probe over the sample. With an advanced control algorithm implemented in a closed-loop feedback system, the setup achieves a position resolution (3 sigma) of 2 nm. The instrument performance is evaluated by 2D fly-scan ptychography with our developed data acquisition strategies. A spatial resolution of 8.8 nm has been demonstrated on a Au test sample with a detector continuous frame rate of 200 Hz. Using a higher flux X-ray source provided by double-multilayer monochromator, we achieve 10 nm resolution for an integrated circuit sample in an ultrafast scan with a detector's full continuous frame rate of 3000 Hz (0.33 ms per exposure), resulting in an outstanding imaging rate of 9 x 10(4) resolution elements per second. (C) 2019 Author(s).

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