Journal
ORGANIC LETTERS
Volume 21, Issue 18, Pages 7509-7513Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b02792
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Funding
- Normandie Universite (NU)
- Region Normandie
- Centre National de la Recherche Scientifique (CNRS)
- Universite de Rouen Normandie (URN)
- INSA Rouen Normandie
- Labex SynOrg [ANR-11-LABX-0029]
- Innovation Chimie Carnot (I2C)
- Institut Universitaire de France
- CNRS Emergence program
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The catalytic asymmetric synthesis of alpha,alpha-difluoromethylated tertiary alcohols is described, using an asymmetric dihydroxylation reaction. This protocol using either the AD-mix-alpha or AD-mix-beta allowed an easy access to these valuable fluorinated chiral building blocks, which have been obtained with excellent yields and er. In addition, the reaction was extended to the alpha-fluoromethylated analogues.
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