Journal
ORGANIC LETTERS
Volume 21, Issue 18, Pages 7386-7389Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b02698
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Funding
- Ministry of Science and Technology of the People's Republic of China [2016YFA0602900]
- National Natural Science Foundation of China [21572071]
- Guangdong Natural Science Foundation [2017A03031-3054]
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A copper-catalyzed cascade cyclization of enynes with Togni's reagent, carbon dioxide, and amines has been successfully developed. The reaction provides a direct and efficient route to a range of trifluoromethyl-substituted carbamates, which are difficult to access using existing methods. Mild reaction conditions, good functional tolerance, and wide substrate scope are the feactures of the protocol.
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