Journal
JOURNAL OF THE TEXTILE INSTITUTE
Volume 111, Issue 4, Pages 597-603Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00405000.2019.1655831
Keywords
Polyethylene terephthalate fiber; carbon microspheres; melamine phosphate; flame retardant
Categories
Funding
- National Natural Science Foundation of China [51302183, U1610255, U1607120, 51603142]
- Natural Science Foundation of Shanxi Province [201801D121096, 2012021021-6, 201801D221129]
- Key Research and Development Program Projects in Shanxi Province [2017030321015-4]
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Carbon microspheres (CMSs) as carbon source, melamine phosphate (MP) as acid source and gas source, the integrated CMSs based MP composites (SiMP-CMSs) was in-situ prepared to improve the flame retardancy of PET fiber. A series of SiMP-CMSs/PET fiber were prepared by the melt spinning method. By investigating the thermal stability, flame retardancy, flame-retardant mode, crystallization and orientation degree of PET composite fiber, the results showed that, with the addition of 0.9 wt% SiMP-CMSs, the LOI value and vertical combustion grade of SiMP-CMSs/PET composite fiber was 27.4% and B1 level. The main flame-retardant mode of SiMP-CMSs/PET fiber was 31.33% physical barrier, 36.04% flame inhibition and 11.12% catalytic charring. The thermal decomposition temperature was delayed, and the residual amount increased from 11.34% to 16.13%. With the accelerated crystallization rate and the increased grain orientation, the aggregated structure of SiMP-CMSs/PET fiber was also optimized.
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