Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 84, Issue 18, Pages 12216-12220Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b01952
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Funding
- SERB New Delhi [EMR/2017/000499]
- University Grants Commission of India (UGC)
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An efficient seven-step, protecting-group-free first total synthesis of chatenaytrienin-2 based on ring-closing metathesis and C(sp)-C(sp(3)) Sonogashira coupling with a 36.5% overall yield has been described. The ready availability of starting materials and key Wittig olefination, ring-closing metathesis, Lindlar reduction, and C(sp)-C(sp(3)) coupling makes this strategy applicable for the synthesis of various unbranched polyene-natural products with 1,5,9,n-(Z)-configured double bonds.
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