Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 84, Issue 19, Pages 12542-12552Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b02042
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Funding
- NSERC [0029322]
- International Research Support Initiative Program (Pakistan)
- SERB Overseas Postdoctoral Fellowship (India)
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Enol ethers are formed by radical decarboxylation of alpha-alkoxy beta-phenylthio acids via the corresponding Barton esters. The phenylthio acids were usually made by the known regioselective reaction of alpha,beta-epoxy acids with PhSH in the presence of InCl3, followed by O-alkylation of the resulting alcohol. In one case, thiol addition to an alpha,beta-unsaturated ethoxymethyl ester was used.
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