Journal
INORGANIC CHEMISTRY
Volume 58, Issue 19, Pages 13376-13381Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.inorgchem.9b02267
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Funding
- NSF [CHE-1506722]
- NIH [101GM128037]
- National Natural Science Foundation of China [21872154]
- Strategic Priority Research Program of the Chinese Academy of Sciences [XDB12010400]
- U.S. National Institutes of Health [R01 CA215157]
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In this work, we present the formation of two open-ended hexagonal-prism tubular macrocycles by the [6 + 12] self-assembly of the symmetric similar to 120 degrees organic ligand donor with similar to 90 degrees Pt(II) acceptor in a 1:2 ratio. The assembled structures were characterized by multinuclear NMR (H-1 NMR, P-31{H-1} NMR, and H-1-H-1 COSY NMR), electrospray ionization mass spectrometry (ESI-TOF-MS), traveling wave ion mobility-mass spectrometry (TWIM-MS), and transmission electron microscopy. Molecular modeling was further conducted to get insight into their structured characteristics. We also examined their photophysical properties.
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