4.5 Article

Pulsed Deposited Manganese and Vanadium Oxide Film Modified with Carbon Nanotube and Gold Nanoparticle: Chitosan and Ionic Liquid-based Biosensor

Journal

ELECTROANALYSIS
Volume 32, Issue 2, Pages 445-453

Publisher

WILEY-V C H VERLAG GMBH
DOI: 10.1002/elan.201900194

Keywords

Gold nanoparticles; manganese and vanadium oxide; pulsed deposition; oxygen; glucose

Funding

  1. Manisa Celal Bayar University Research Foundation [2017-018]

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Present study describes the synthesis of mixed oxide films of manganese and vanadium by electrochemical pulsed deposition technique on a glassy carbon electrode (GCE) modified with multiwall carbon nanotubes (MWCNT). The film was further decorated with gold nanoparticles to enhance the reduction signal of dissolved oxygen in pH 5.17 acetate buffer solution. All of the electrochemical synthesized modified electrodes have been characterized with Scanning electron microscopy(SEM), High-resolution transmission electron microscopy (HRTEM), X-Ray photoelectron spectroscopy (XPS), X-Ray diffraction (XRD) techniques. The electrode obtained (AuNPs/MnOx-VOx/CNT/GCE) was utilized as a platform for glucose biosensor where the glucose oxidase enzyme was immobilized on the composite film with the aid of chitosan and an ionic liquid. The electrochemical performance of the biosensor was investigated by cyclic voltammetry and the relative parameters have been optimized by amperometric measurements in pH 5.17 acetate buffer solution. The developed biosensor exhibited a linear range for glucose between 0.1-1.0 mM and the limit of detection was calculated as 0.02 mM.

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