4.7 Article

Nano-infiltration and transient eutectic (NITE) phase joining SiC ceramics at 1500°C

Journal

CERAMICS INTERNATIONAL
Volume 45, Issue 18, Pages 24927-24931

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2019.08.193

Keywords

SiC joining; NITE-Phase; CeO2-Al2O3; Low-temperature joining; Microstructure; Shear strength

Funding

  1. Pearl River Nova Program of Guangzhou [201710010142]
  2. Science and Technology Planning Project of Guangdong Province [2017A050501033]
  3. National Natural Science Foundation of China [51402055, 51602060, U1401247]
  4. Guangdong Innovative and Entrepreneurial Research Team Program [2013G061, 2014YT02C049]
  5. National Major Science and Technology Projects of China [2015ZX06004001]
  6. National Key R&D Program of China [2017YFB0702404]

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By using nano-infiltration and transient eutectic (NITE) phase with nanosized SiC and the addition of CeO2-Al2O3 as joining material, liquid-phase-sintered SiC ceramics were joined at the relatively low temperature of 1500 degrees C and 1700 degrees C. For comparison purpose, Al2O3-Y2O3 and SiO2-Al2O3-Y2O3 were used as the additives to join SiC ceramics. The shear strength of SiC assembly with the interlayer thickness of similar to 70 mu m and addition of CeO2-Al2O3 after joining at 1700 degrees C was measured to be 163.9 MPa but decreased to 57.4 MPa when joining at 1500 degrees C. It was revealed that the joining status could be improved by decreasing the thickness of the interlayer to similar to 35 mu m and SiC joint finishing at 1500 degrees C possessed the comparatively high shear strength of 113.2 MPa. NITE phase containing other additives (Al2O3-Y2O3 and SiO2-Al2O3-Y2O3) showed the much lower shear strength after joining at 1500 degrees C.

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