4.4 Article

Electrochemical Determination of Sesamol in Foods by Square Wave Voltammetry at a Boron-Doped Diamond Electrode

Journal

ANALYTICAL LETTERS
Volume 53, Issue 3, Pages 343-354

Publisher

TAYLOR & FRANCIS INC
DOI: 10.1080/00032719.2019.1650752

Keywords

Boron-doped diamond electrode (BDDE); cyclic voltammetry (CV); sesamol; square wave voltammetry (SWV); tahini halva

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Sesamol is a phenolic compound naturally found in sesame seeds. It has beneficial health effects in humans, as it features significant antioxidant activity and has anticancer and anti-aging properties. Therefore, finding a suitable electrode surface for sesamol determination is important. The prominent advantage of boron-doped diamond electrodes is their use in many sensing platforms without the need for the surface modification. This study represents the first time that sesamol has been determined using boron-doped diamond electrodes in acidic media by square wave voltammetry. Linear responses of sesamol were obtained in the concentration range from 0.2 mu M to 1000 mu M, and the detection limit was determined to be 85 nM based on a signal-to-noise ratio of 3. The relative standard deviations were 2.1% for a 1 mu M standard with three measurements.

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