Journal
CHEMELECTROCHEM
Volume 6, Issue 13, Pages 3383-3386Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/celc.201900753
Keywords
electro-oxidative; [3+2] annulation; 1; 3-dicarbonyl compounds; dihydrofuran; 1; 1; 1; 3; 3; 3-hexafluoro-2-propanol
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Funding
- National Natural Science Foundation of China [21520102003, 21532005]
- Hubei Province Natural Science Foundation of China [2017CFA010]
- Program of Introducing Talents of Discipline to Universities of China (111 Program)
- China State Key Research Grant [2016YEF0200503]
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: A straightforward and atom-economical approach to the synthesis of dihydrofurans employing electro-oxidative [3+2] annulation of 1,3-dicarbonyl compound and alkenes has been developed. Neither metal catalysts nor chemical oxidants are required to promote the dehydrogenation process. Moreover, the use of base to decrease the oxidative potential and 1,1,1,3,3,3-hexafluoro-2-propanol to stabilize the reactive intermediates are key to the success of the cyclization.
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