4.6 Article

Complex Study of Eutectoidal Phase Transformation of 2507-Type Super-Duplex Stainless Steel

Journal

MATERIALS
Volume 12, Issue 13, Pages -

Publisher

MDPI
DOI: 10.3390/ma12132205

Keywords

duplex stainless steel; eutectoidal decomposition; cold rolling; heat treatment; magnetic testing; thermoelectric power; EBSD; activation energy

Funding

  1. Higher Education Excellence Program of the Ministry of Human Capacities in the frame of nanotechnology research area of Budapest University of Technology and Economics (BME FIKP-NAT)

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The aim of this work was to study expansively the process of the eutectoidal phase transformation of 2507-type super-duplex stainless steel. Three sample sets were prepared. The first sample set was made to investigate the effect of the previous cold rolling and heat treatment for the eutectoidal phase transformation. Samples were cold rolled at seven different rolling reductions which was followed by heat treatment at five different temperatures. The second sample set was prepared to determine the activation energy of the eutectoidal decomposition process using the Arrhenius equation. Samples were cold rolled at seven different rolling reductions and were heat treated at the same temperature during eight different terms. A third sample set was made to study how another plastic-forming technology, beside the cold rolling, can influence the eutectoidal decomposition. Samples were elongated by single axis tensile stress and were heat treated at the same temperature. The results of the first and the third sample sets were compared. The rest delta-ferrite contents were calculated using the results of AC and DC magnetometer measurements. DC magnetometer was used as a feritscope device in this work. Light microscope and electron back scattering diffraction (EBSD) images demonstrated the process of the eutectoidal decomposition. The thermoelectric power and the hardness of the samples were measured. The results of the thermoelectric power measurement were compared with the results of the delta-ferrite content measurement. The accurate value of the coercive field was determined by a Foerster-type DC coercimeter device.

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