Journal
ORGANIC LETTERS
Volume 21, Issue 14, Pages 5500-5504Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b01804
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Funding
- Natural Science Basic Research Plan in Shaanxi Province of China [2019JM-299]
- Key Laboratory Construction Program of Van Municipal Bureau of Science and Technology [201805056ZD7CG40]
- Fundamental Research Funds of the Central Universities [zrzd2017001, xjj2016056, xzy022019039]
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A visible-light-driven sulfamate esters guided alkylation of unactivated C(sp(3))-H bonds enabled by a 1,6-HAT/radical addition cascade is described. Not only structurally diverse Michael acceptors but also styrenes are amenable to this alkylation reaction. Notably, the N-H bonds activation radical relay refrained from prefunctionalization and using excess external oxidants.
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