Journal
ORGANIC LETTERS
Volume 21, Issue 13, Pages 5326-5330Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b01941
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Funding
- Austrian COMET Program by the Austrian Federal Ministry of Transport, Innovation and Technology (BMVIT) [862766]
- Austrian Federal Ministry of Digital and Economic Affairs (BMDW)
- State of Styria (Styrian Funding Agency SFG)
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A continuous process for the on-demand generation, separation, and reaction of hydrogen cyanide (HCN) using membrane separation technology was developed. The inner tube of the reactor is manufactured from a gas-permeable, hydrophobic fluoropolymer (Teflon AF-2400) membrane. HCN is formed from aqueous reagents within the inner tube and then diffuses through the membrane into an outer tubing containing organic solvent. This technique enabled the safe handling of HCN for three different organic transformations without the need for distillation.
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