Journal
ORGANIC LETTERS
Volume 21, Issue 14, Pages 5606-5610Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b01954
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- CSIR, New Delhi [02(0307)/17/EMR-II]
- UGC-New Delhi (UGC-SRF)
- CSIR-New Delhi (CSIR-SRF)
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A mild and efficient method for the direct difluoromethylenephosphonation of imidazopyridines has been developed using rose bengal (RB) as a photoredox catalyst. Bis(pinacolato)diboron (B(2)pin(2)) is found to be a crucial additive in the present reaction. The present methodology is also applicable to other heterocycles like imidazo[2,1-b]thiazole, benzo[d]imidazo-[2,1-b]thiazole, and indole. The reaction possibly proceeds through a single electron transfer (SET) process.
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