Journal
ORGANIC LETTERS
Volume 21, Issue 17, Pages 6585-6588Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b02069
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Funding
- JSPS KAKENHI [JP22390002, JP24106731, JP16H01157, JP26293004, JP17K14449, JP18H04418, JP18H04624, JP18H02557]
- Asahi Glass Foundation
- MEXT Project of Integrated Research Consortium on Chemical Sciences
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Herein, we report a double deprotonation method used for the preparation of ynolates starting from nonbrominated 2,6-di-tertbutylphenyl esters. The current method is superior to the previously described double lithium/halogen exchange approach because easily accessible starting materials are used. This method will be especially useful for preparation of ynolates bearing functional groups in organic synthesis.
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