Journal
MICROCHEMICAL JOURNAL
Volume 147, Issue -, Pages 163-169Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.microc.2019.02.067
Keywords
Nickel nanoparticles; Graphene foam; Chemical vapor deposition; Levodopa; Uric acid
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Funding
- Technology Foundation for Selected Overseas Chinese Scholar, Ministry of Personnel of China [2015192]
- Postdoctoral Initial Founding of Heilongjiang Province [LBH-Q14117]
- Innovative Talent Fund of Harbin City [2016RAQXJ185]
- Science Funds for the Young Innovative Talents of HUST [201604]
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Spherical nickel nanoparticles were prepared by an N2H4-based solution reduction route. Then, graphene was deposited on the template of nickel nanoparticles by chemical vapor deposition (CVD) at a high temperature. After etching nickel, small-sized, porous and free-standing 3D graphene foam (3D GF) was obtained. It was transferred on the indium tin oxide (ITO) glass (3D GF/ITO) for electrochemical determination of levodopa in the presence/absence of uric acid. The results show that the pore size of the 3D GF is similar to 1 mu m. The electrode shows a high sensitivity of 0.24 mu A.mu M-1 for the detection of levodopa. The electrode also shows a low measured limit of detection, superior selectivity, reproducibility and stability. Meanwhile, it shows a great potential in the clinical application.
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