Journal
JOURNAL OF THE AMERICAN CERAMIC SOCIETY
Volume 102, Issue 11, Pages 6475-6479Publisher
WILEY
DOI: 10.1111/jace.16702
Keywords
fluorine; fluorine compounds; nanomaterials; solvothermal synthesis
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Funding
- Korea Government (MSIT) [2017R1C1B2005403]
- National Research Foundation of Korea [2017R1C1B2005403] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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In this study, we have developed a simple, versatile, and rapid solvothermal process for the preparation of sodium metal fluoride (NaxMFy) nanopowders (NaCoF3, NaMnF3, and Na3FeF6) using a microwave digestion system. Microwave heating significantly reduces the reaction time compared to conventional heating methods. The NaxMFy nanopowders have cluster structures consisting of small primary nanoparticles, thus resulting in a large surface area of >60 m(2) g(-1). The effect of an essential additive is also investigated to confirm the optimal conditions for obtaining large-surface-area NaxMFy nanopowders without impurities. We expect that this study will promote further research into the development and application of various nanostructured NaxMFy materials.
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