Journal
JOURNAL OF NATURAL PRODUCTS
Volume 82, Issue 8, Pages 2291-2298Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.jnatprod.9b00504
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Funding
- University of Auckland
- New Zealand Foundation for Research Science and Technology [CO1X0205]
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An acetylenic 2-amino-3-alcohol, distaminolyne B (2), isolated from the New Zealand ascidian Pseudodistoma cereum, is reported. The isolation and structure elucidation of 2 and assignment of 2S,3S absolute configuration (AC) using the exciton coupled circular dichroism technique are described. Using a methodologically facile workflow, the same AC was also established by analysis of specific rotation, terminal methyl C-1 delta(C) chemical shift, and NH delta(H) and J values of the N,O-diacetate derivative.
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