Journal
APPLIED SCIENCES-BASEL
Volume 9, Issue 6, Pages -Publisher
MDPI
DOI: 10.3390/app9061100
Keywords
solvothermal method; NiCo2O4; mesoporous nanostructures; catalytic properties; thermal decomposition
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Funding
- Natural Science Foundation of Fujian Province [2017J01676]
- Key Research Foundation for Young Scholars of Fujian Education Department of China [JZ160486, JZ160484]
- Program for New Century Excellent Talents in Fujian Province University (Minjiaoke [2018]) [47]
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In this paper, we prepared mesoporous nickel cobaltite (NiCo2O4) nanostructures with multi-morphologies by simple solvothermal and subsequent heat treatment. By adjusting the solvent type, mesoporous NiCo2O4 nanoparticles, nanorods, nanowires, and microspheres were easily prepared. The as-prepared products were systematically characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), and Brunauer-Emmett-Teller (BET) method. Furthermore, the catalytic activities towards the thermal decomposition of ammonium perchlorate (AP) of as-prepared NiCo2O4 nanostructures were investigated.
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