4.6 Article

Preparation and Short-Term Aging Properties of Asphalt Modified by Novel Sustained-Release Microcapsules Containing Rejuvenator

Journal

MATERIALS
Volume 12, Issue 7, Pages -

Publisher

MDPI
DOI: 10.3390/ma12071122

Keywords

modified asphalt; sustained-release microcapsules; rejuvenator; aging properties

Funding

  1. International Project on Scientific and Technological Cooperation in the Shaanxi Province of China [2018KW-052]
  2. State Key Laboratory of High Performance Civil Engineering Materials [2018CEM010]
  3. Fundamental Research Funds for the Central Universities of China [300102318402, 300102219509]

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Aged asphalt can enormously affect the performance of asphalt pavement and cause serious environmental hazards. Microcapsule-modified asphalt is one of the effective means to improve the anti-aging ability of asphalt. In this work, novel sustained-release microcapsules containing rejuvenator were prepared by the solvent evaporation method. The morphology of the microcapsules was characterized by scanning electron microscopy (SEM). The sustained-release properties of the microcapsules were investigated by static thermogravimetric analysis. The physical properties such as penetration, ductility, softening point, and Brookfield viscosity of the original asphalt and microcapsule-modified asphalt were studied. In addition, the viscoelasticity of the original asphalt and microcapsule-modified asphalt was investigated by means of a dynamic shear rheometer (DSR). The results show that the prepared microcapsules have a smooth surface and a complete encapsulation with an average particle size of 60 m. After the heating treatment (above 140 degrees C), a large number of micropores were formed on the shell surface of microcapsules, which provided a structural basis for the sustained-release of rejuvenator. The release rate of the rejuvenator was obviously slowed down by the microcapsules. The aging behavior of sustained-release microcapsules containing rejuvenator-modified asphalt can be greatly improved. The enhanced anti-aging properties of sustained-release microcapsule-modified asphalt are attributed to the functions of the rejuvenator which can be slowly released from the micropores on the microcapsules' surface, after which the light components lost in the original asphalt can be supplemented.

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