Journal
ACS CATALYSIS
Volume 9, Issue 7, Pages 5897-5901Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acscatal.9b01921
Keywords
carboxylation; nickel; isotopic labeling; carbon dioxide; carboxylic acid
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Funding
- ICIQ European Research Council [ERC-PoC-2016-755251]
- MINECO [CTQ2015-65496-R]
- MECD (FPU program)
- China Scholarship Council (CSC)
- European Union's Horizon 2020 under the Marie Sklodowska-Curie grant [795961]
- Marie Curie Actions (MSCA) [795961] Funding Source: Marie Curie Actions (MSCA)
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An integrated catalytic decarboxylation/carboxylation for accessing isotopically labeled carboxylic acids with (CO2)-C-13 or (CO2)-C-14 is described. The method shows a wide scope under mild conditions, even in the context of late-stage functionalization, and does not require stoichiometric organo-metallics, thus complementing existing carbon-labeling techniques en route to carboxylic acids.
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