4.7 Article

Magnesium alloy ZK60 tubing made by Shear Assisted Processing and Extrusion (ShAPE)

Publisher

ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2019.04.013

Keywords

ShAPE; Friction extrusion; Friction stir extrusion; Friction stir back extrusion; Magnesium; Grain refinement

Funding

  1. U.S. Department of Energy Vehicle Technologies Office (DOE/VTO)
  2. MS3 (Materials Synthesis and Simulation Across Scales) Initiative at Pacific Northwest National Laboratory
  3. United States Department of Energy [DE-AC06-76LO1830]

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ZK60 Magnesium tubing has been friction extruded from as-cast billets and T5 conditioned bars using Shear Assisted Processing and Extrusion (ShAPE). Tubes having an outer diameter of 50.8 mm and wall thickness of 1.9 mm were extruded with > 20 times less ram force compared to conventional extrusion due to the unique shearing conditions and tooling inherent to ShAPE. Microstructures of the as-cast billet and T5 bar feedstock materials were significantly different from each other in terms of grain size, texture, and second phase distribution; yet the resulting microstructures after ShAPE were remarkably similar. An average grain size of 4-5 mu m, 20 degrees tilt of basal texture away from the extrusion axis, and refined second phases having a uniform distribution were achieved independent of the feedstock material. Hardness for as-extruded and artificially aged tubes are presented with isotropic behavior explained by detailed microstructural analysis. This work suggests that bulk ZK60 magnesium alloys extrusions may be fabricated in a single step, with microstructures that are unobtainable with conventional extrusion.

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