Journal
JOURNAL OF STRUCTURAL CHEMISTRY
Volume 60, Issue 2, Pages 279-283Publisher
PLEIADES PUBLISHING INC
DOI: 10.1134/S0022476619020136
Keywords
copper(II) complexes; crystal structure; coordination polymers; chiral complexes; malic acid
Funding
- RFBR [18-29-04001]
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The [Cu-8(S-mal)(4)(bptc)(H2O)(12)] 0.5H(4)bptc 7.5H(2)O coordination polymer is obtained by heating the copper(II) nitrate, S-malic acid (H(3)mal), and biphenyl-3,3,5,5-tetracarboxylic (H(4)bptc) acid solution in the water-N,N-diethylformamide mixture. The crystal structure is determined from XRD data. The compound has a three-dimensional homochiral framework with channels filled by crystallization molecules of tetracarboxylic acid and water. The composition and structure of the coordination polymer obtained are confirmed by X-ray powder diffraction, IR spectroscopy, thermogravimetric analysis, and elemental analysis.
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